1. Identity and material

Botanical name: Asparagus racemosus Willd. Plant part: root (tuberous root, dried). Preparation: dry extract; extraction solvent and herb-to-extract ratio stated by the supplier. Carriers: declared by name and percentage, or “none”. Identity test: TLC or HPTLC profile to comply with an A. racemosus root reference standard, all major bands.

Why: the binomial and the plant part are the two clauses most often missing from a supplier sheet, and the two that decide whether a substitute passes. See adulteration and authenticity.

2. Assay

Primary: total saponins by gravimetry, on a dry-weight basis, NLT 20.0 / 40.0 / 60.0% w/w according to grade, batch result printed as a number. Secondary: shatavarin IV by HPLC, reported per lot as a number against a stated reference standard; if you need a minimum, agree it with the supplier on a current lot before writing it in. Method statement: the method must appear on the COA next to the result.

Why: gravimetric is the trade basis; HPLC is the orthogonal check. Writing both prevents a gravimetric number being presented against an HPLC expectation, and vice versa.

3. Physical parameters

ClauseTypical limitMethod
AppearanceLight brown to brown, free-flowing powderVisual
Loss on dryingNMT 6.0% w/w (EU grade) or NMT 10.0%USP <731>
Bulk density0.30 to 0.80 g/mLUSP <616>
Water-soluble extractiveNLT 70.0% w/wUSP <561>
Particle sizeNLT 95% through #40 meshUSP <786>
Total ashNMT 10.0% w/wUSP <561> or IP

4. Contaminants

Heavy metals by ICP-MS as numbers: lead, cadmium, mercury, arsenic, with limits chosen for the destination (EU supplement ceilings of Pb 3.0, Cd 1.0, Hg 0.1 ppm; many buyers write Pb 1.0 and As 1.0). Pesticide residues: multi-residue screen by LC-MS/MS and GC-MS/MS reported against Regulation (EC) 396/2005 MRLs, limit of quantification stated. Ethylene oxide (sum expressed as ETO) with LOQ. PAH: benzo(a)pyrene and PAH4 against the EU contaminant regulation. Aflatoxins: B1 and total by HPLC-FLD. Residual solvents: USP <467> or the EU extraction-solvent directives.

Why: this block is what separates an EU-grade lot from a standard one, and its cost and lead time belong in the quotation. Write it into the specification only for the row you intend to buy.

5. Microbiology

Total aerobic count NMT 1,000 or 10,000 cfu/g; yeast and mould NMT 100 or 1,000 cfu/g; E. coli absent per 10 g; Salmonella absent per 25 g; S. aureus absent; methods named (USP <2021>, <2022>). Add a retest clause for lots older than six months at shipment if your application is sensitive.

6. Declarations and documents

Non-irradiated, non-ETO treated, GMO-free, allergen statement, vegan, BSE/TSE-free. Documents per lot: COA with batch number, specification, SDS, allergen statement, certificate of origin, phytosanitary certificate where required, and on request the HPLC report with chromatogram and a third-party residue report with the laboratory named. Certificates of the manufacturing facility with validity dates.

7. Packaging, storage and shelf life

25 kg HDPE drum with double PE liner unless agreed otherwise; store cool and dry, sealed, away from light; shelf life 36 months from manufacture unopened, with the basis for the claim available on request.

8. Commercial clauses that belong in the specification

Our own published specification for the 20% EU grade follows this structure and can be used as the starting document. Send us yours and we return it marked up, clause by clause, against the current lot.